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Dauphiné twinning and texture memory in polycrystalline quartz. Part 1: Experimental deformation of novaculite

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Abstract

Mechanical Dauphiné twinning in quartz has been of long-standing interest, both in single crystals and polycrystalline aggregates. This study investigates texture development in fine-grained quartz rock novaculite with no initial texture using compression experiments conducted in the Paterson gas apparatus to explore the influence of stress and temperature. Texture patterns are measured with time-of-flight neutron diffraction and hard synchrotron X-rays, analyzing diffraction data with the Rietveld method. Similar texture patterns are observed as described previously but the new results establish a profound influence of temperature and document that twinning initiates at stresses less than 50 MPa. Possibilities of using Dauphiné twinning as a paleopiezometer in quartz-bearing rocks are discussed.

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References

  • Baker DW, Wenk H-R (1972) Preferred orientation in a low symmetry quartz mylonite. J Geol 80:81–105

    Article  Google Scholar 

  • Barber DJ, Wenk H-R (1991) Dauphiné twinning in deformed quartzites: implications of an in situ TEM study of the α–β phase transformation. Phys Chem Miner 17:492–502

    Article  Google Scholar 

  • Barton NR, Benson DJ, Becker R (2005) Crystal level continuum modelling of phase transformations: the α↔ε transformation in iron. Model Simul Mater Sci Eng 13:707–731

    Article  Google Scholar 

  • Bishop JR (1981) Piezoelectric effects in quartz-rich rocks. Tectonophysics 77:297–321

    Article  Google Scholar 

  • Frondel C (1945) Secondary Dauphiné twinning in quartz. Am Mineral 30:447–461

    Google Scholar 

  • Frondel C (1962) The system of mineralogy, 7th edn, vol 3. Wiley, New York

  • Ghomshei MM, Templeton TL (1989) Piezoelectric and a-axis fabric along a quartz vein. Phys Earth Planet Int 55:374–386

    Article  Google Scholar 

  • Hammersley AP (1998) Fit2D: V99.129 reference manual, version 3.1. Internal Report ESRF-98-HA01

  • Heaney PJ, Veblen DR (1991) Observation and kinetic analysis of a memory effect at the α–β quartz transition. Am Mineral 76:1459–1466

    Google Scholar 

  • Heaney PJ, Prewitt CT, Gibbs GV (1994) Silica. Physical behavior, geochemistry and materials applications. Rev Mineral Min Soc Am 29:606

    Google Scholar 

  • Heidelbach F, Kunze K, Wenk H-R (2000) Texture analysis of a recrystallized quartzite using electron diffraction in the scanning electron microscope. J Struct Geol 22:91–104

    Article  Google Scholar 

  • Ischia G, Wenk H-R, Lutterotti L, Berberich F (2005) Quantitative Rietveld texture analysis of zirconium from single synchrotron diffraction images. J Appl Cryst 38:377–380

    Article  Google Scholar 

  • Klassen-Neklyudova MV (1964) Mechanical twinning of crystals (translated from Russian by JES Bradley). Consultants Bureau, New York, p 213

  • Larson AC, Von Dreele RB (2004) General structure analysis system (GSAS). Los Alamos National Laboratory Report LAUR 86-748

  • Lloyd GE (2000) Grain boundary contrast effects during faulting of quartzite: an SEM/EBSD analysis. J Struct Geol 22:1675–1693

    Article  Google Scholar 

  • Lloyd GE (2004) Microsturctural evolution in a mylonitic quartz simple shear zone: the significant roles of dauphine twinning and misorientation. In: Alsop GI et al (eds) Transports and flow processes in shear zones. Geological Society of London, Special Publication, vol 224, pp 39–61

  • Lonardelli I, Wenk H-R, Lutterotti L, Goodwin M (2005) Texture analysis from synchrotron diffraction images with the Rietveld method: dinosaur tendon and salmon scale. J Synchrotron Rad 12:354–360

    Article  Google Scholar 

  • Lutterotti L, Matthies S, Wenk H-R (1999) MAUD: a friendly Java program for materials analysis using diffraction. Int Union Crystallogr Comm Powder Diffr Newsl 21:14–15

    Google Scholar 

  • Markgraaf J (1986) Elastic behavior of quartz during stress-induced Dauphiné twinning. Phys Chem Miner 13:102–112

    Article  Google Scholar 

  • Matthies S, Vinel GW (1982) On the reproduction of the orientation distribution function of textured samples from reduced pole figures using the concept of conditional ghost correction. Physica Status Solidi B 112:K111–K114

    Google Scholar 

  • McLellan AG (1978) The thermodynamic theory of the growth of Dauphiné twinning in quartz under stress. J Phys C 11:4665–4679

    Article  Google Scholar 

  • Ohno I (1995) Temperature variation of elastic properties of α-quartz up to the α–β transition. J Phys Earth 43:157–169

    Google Scholar 

  • Ohno I, Harada K, Yoshitomi C (2006) Temperature variation of elastic constants of quartz across the α–β transition. Phys Chem Miner 33:1–9

    Article  Google Scholar 

  • Parkhomenko EI (1971) Electrification phenomena in rocks. (Translation by GV Keller). Plenum Press, New York, 285 pp

  • Paterson MS (1970) A high-pressure, high-temperature apparatus for rock deformation. Int J Rock Mech Mining Sci Geomech Abstr 7:517–526

    Article  Google Scholar 

  • Pehl J, Wenk H-R (2005) Evidence for regional Dauphiné twinning in quartz from the Santa Rosa mylonite zone in Southern California. A neutron diffraction study. J Struct Geol 27:1741–1749

    Article  Google Scholar 

  • Sander B (1950) Einführung in die Gefügekunde der geologischen Körper. Springer, Vienna

    Google Scholar 

  • Schmidt W (1925) Gefügestatistik. Tschermaks Mineral Petrog Mitt 38:392–423

    Google Scholar 

  • Schubnikov A, Zinserling K (1932) Ueber die Schlag- und Druckfiguren und ueber die mechanische Quartzzwillinge. Z Kristallogr 83:243–264

    Google Scholar 

  • Smirnov MB, Mirgorodsky AP (1997) Lattice-dynamical study of the α–β phase transition of quartz: soft-mode behavior and elastic anomalies. Phys Rev Lett 78:2413–2416

    Article  Google Scholar 

  • Sorrell AC, Anderson HU, Ackermann RJ (1974) Thermal expansion and the high-low transformation in quartz. II. Dilatometric studies. J Appl Cryst 7:468–473

    Article  Google Scholar 

  • Sosman RB (1965) The phases of silica. Rutgers University Press, New Brunswick, 388 pp

  • Thomas LA, Wooster WA (1951) Piezocrescence—the growth of Dauphiné twinning in quartz under stress. Proc R Soc Lond A 208:43–62

    Article  Google Scholar 

  • Trepmann CA, Spray JG (2005) Planar microstructures and Dauphiné twins in shocked quartz from the Charlevoix impact structure, Canada. Geol Soc Am Spec Pap 384:315–328

    Google Scholar 

  • Trimby PW, Prior DJ, Wheeler J (1998) Grain boundary hierarchy development in a quartz mylonite. J Struct Geol 20:917–935

    Article  Google Scholar 

  • Tullis J (1970) Quartz: preferred orientation in rocks produced by Dauphiné twinning. Science 168:1342–1344

    Article  Google Scholar 

  • Tullis TE (1980) The use of mechanical twinning in minerals as a measure of shear stress magnitudes. J Geophys Res 85:6263–6268

    Article  Google Scholar 

  • Tullis J, Tullis TE (1972) Preferred orientation produced by mechanical Dauphiné twinning. Thermodynamics and axial experiments. Am Geophys U Monogr 16:67–82

    Google Scholar 

  • Van Groos AFK, Heege JPT (1973) The high-low quartz transition up to 10 kb pressure. J Geol 81:717–724

    Google Scholar 

  • Van Tendeloo G, Van Landuyt J, Amelickx S (1976) The α–β phase transition in quartz and AlPO4 as studied by electron microscopy and diffraction. Physica Status Solidi A 33:723–735

    Google Scholar 

  • Wenk H-R, Grigull S (2003) Synchrotron texture analysis with area detectors. J Appl Cryst 36:1040–1049

    Article  Google Scholar 

  • Wenk H-R, Lutterotti L, Vogel S (2003) Texture analysis with the new HIPPO TOF diffractometer. Nuclear Instrum Methods A515:575–588

    Google Scholar 

  • Wenk H-R, Lonardelli I, Vogel SC, Tullis J (2005) Dauphiné twinning as evidence for an impact origin of preferred orientation in quartzite: an example from Vredefort, South Africa. Geology 33:273–276

    Article  Google Scholar 

  • Wooster WA, Wooster N (1946) Control of electrical twinning in quartz. Nature 157:405–406

    Google Scholar 

  • Wooster WA, Wooster N, Rycroft JL, Thomas LA (1947) The control and elimination of electrical (Dauphiné) twinning in quartz. J Inst Electr Eng 94:927–938

    Google Scholar 

  • Zinserling KV (1961) Artificial twinning of quartz (in Russian). Acad Sci USSR Moscow

Download references

Acknowledgments

We are appreciative to M. Naumann, S. Gehrmann and K. Peach for help with deformation experiments and sample preparation. Jan Tullis provided some of the samples and inspiring discussions. Comments from a reviewer were most helpful. Texture measurements were performed at synchrotron beamlines PETRA2 at HASYLAB 6 (DESY) and ID 15B of ESRF. Some samples were also measured by neutron diffraction with HIPPO at LANSCE with the help of Sven Vogel. HRW is grateful for hospitality at the GeoForschungsZentrum Potsdam during a sabbatical leave. The work of NB was performed under the auspices of the U.S. Department of Energy by University of California, Lawrence Livermore National Laboratory under Contract W-7405-Eng-48 (UCRL-JRNL-220357). Research was supported by NSF (EAR 0337006) and DOE (DE-FG02-05ER15637).

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Correspondence to Hans-Rudolf Wenk.

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Wenk, HR., Rybacki, E., Dresen, G. et al. Dauphiné twinning and texture memory in polycrystalline quartz. Part 1: Experimental deformation of novaculite. Phys Chem Minerals 33, 667–676 (2006). https://doi.org/10.1007/s00269-006-0115-9

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  • DOI: https://doi.org/10.1007/s00269-006-0115-9

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